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25 Advanced Solved Numericals on Ionic Equilibrium

25 Advanced Solved Numericals on Ionic Equilibrium | Chemca

Masterclass: 25 Solved JEE Advanced Numericals on Ionic Equilibrium

Conquer the complexities of acids, bases, and salts! This exhaustive guide features highly rigorous multi-step problems on Buffer Solutions, Salt Hydrolysis, Solubility Products, and the exact pH of dilute solutions. Click "View Solution" to reveal the step-by-step breakdown.

Problem 1: Exact pH of Extremely Dilute Strong Acid
Calculate the exact pH of a $1.0 \times 10^{-8} \text{ M}$ aqueous solution of Hydrochloric acid ($HCl$) at $298 \text{ K}$.
View Solution

Step 1: Understand the Trap
A common mistake is taking $pH = -\log_{10}(10^{-8}) = 8$. An acid can NEVER have a basic pH (> 7) at $298 \text{ K}$. At such low concentrations, the $H^+$ contributed by the auto-ionization of water cannot be ignored.

Step 2: Setup the Equations
Let the concentration of $H^+$ from water be $x \text{ M}$.
Therefore, $[OH^-] = x \text{ M}$.
Total $[H^+] = 10^{-8} \text{ (from HCl)} + x \text{ (from water)}$.

Step 3: Apply the Ionic Product of Water ($K_w$)
$K_w = [H^+][OH^-] = 1.0 \times 10^{-14}$
$(10^{-8} + x)(x) = 10^{-14}$
$x^2 + 10^{-8}x - 10^{-14} = 0$

Step 4: Solve the Quadratic Equation
$x = \frac{-10^{-8} + \sqrt{(10^{-8})^2 - 4(1)(-10^{-14})}}{2}$
$x = \frac{-10^{-8} + \sqrt{10^{-16} + 4 \times 10^{-14}}}{2} = \frac{-10^{-8} + \sqrt{401 \times 10^{-16}}}{2}$
$x = \frac{-10^{-8} + 20.02 \times 10^{-8}}{2} = \frac{19.02 \times 10^{-8}}{2} = 9.51 \times 10^{-8} \text{ M}$.

Step 5: Calculate Final pH
Total $[H^+] = 10^{-8} + 9.51 \times 10^{-8} = 10.51 \times 10^{-8} = 1.051 \times 10^{-7} \text{ M}$.
$pH = -\log_{10}(1.051 \times 10^{-7}) = 7 - \log_{10}(1.051) = 7 - 0.021 = 6.98$.

Answer: The exact pH is $6.98$.
Problem 2: Weak Acid Dissociation and Approximation
A $0.1 \text{ M}$ solution of Acetic acid ($CH_3COOH$) has a dissociation constant $K_a = 1.8 \times 10^{-5}$. Calculate its degree of dissociation ($\alpha$) and the pH of the solution.
View Solution

Step 1: Check Approximation Validity
Ostwald's dilution law: $K_a = \frac{C\alpha^2}{1-\alpha}$.
If $K_a \le 10^{-4}$ and $C$ is relatively large ($0.1 \text{ M}$), $\alpha$ is very small, so $1 - \alpha \approx 1$.
$K_a \approx C\alpha^2 \implies \alpha = \sqrt{\frac{K_a}{C}}$.

Step 2: Calculate $\alpha$
$\alpha = \sqrt{\frac{1.8 \times 10^{-5}}{0.1}} = \sqrt{1.8 \times 10^{-4}} = \sqrt{1.8} \times 10^{-2}$.
Since $\sqrt{1.8} \approx 1.34$, $\alpha = 1.34 \times 10^{-2}$ or $1.34\%$. (Approximation is highly valid since $\alpha < 5\%$).

Step 3: Calculate pH
$[H^+] = C\alpha = 0.1 \times 1.34 \times 10^{-2} = 1.34 \times 10^{-3} \text{ M}$.
Alternatively: $[H^+] = \sqrt{K_a C} = \sqrt{1.8 \times 10^{-5} \times 0.1} = \sqrt{18 \times 10^{-7}} = \sqrt{1.8 \times 10^{-6}} = 1.34 \times 10^{-3} \text{ M}$.
$pH = -\log_{10}(1.34 \times 10^{-3}) = 3 - \log_{10}(1.34) = 3 - 0.127 = 2.87$.

Answer: $\alpha = 0.0134$ ($1.34\%$); $pH = 2.87$.
Problem 3: Mixture of Two Weak Acids
Calculate the $[H^+]$ in a solution containing $0.1 \text{ M}$ Formic acid ($HCOOH$, $K_{a1} = 1.8 \times 10^{-4}$) and $0.2 \text{ M}$ Acetic acid ($CH_3COOH$, $K_{a2} = 1.8 \times 10^{-5}$).
View Solution

Step 1: Understand Isohydric Solutions
When two weak acids are mixed, they mutually suppress each other's dissociation due to the common ion effect of $H^+$. The total $[H^+]$ is the sum of contributions from both acids.

Step 2: Apply the Mixture Formula
For a mixture of two weak acids with concentrations $C_1$ and $C_2$, the total $H^+$ concentration is given by:
$[H^+] = \sqrt{K_{a1}C_1 + K_{a2}C_2}$

Step 3: Substitute and Solve
$[H^+] = \sqrt{(1.8 \times 10^{-4} \times 0.1) + (1.8 \times 10^{-5} \times 0.2)}$
$[H^+] = \sqrt{(1.8 \times 10^{-5}) + (0.36 \times 10^{-5})}$
$[H^+] = \sqrt{2.16 \times 10^{-5}} = \sqrt{21.6 \times 10^{-6}}$
$[H^+] = 4.65 \times 10^{-3} \text{ M}$.

Answer: $[H^+] = 4.65 \times 10^{-3} \text{ M}$.
Problem 4: Polyprotic Acids and Secondary Ions
In a $0.1 \text{ M}$ solution of $H_2S$, calculate the concentration of $S^{2-}$ ions. Given $K_{a1} = 1.0 \times 10^{-7}$ and $K_{a2} = 1.2 \times 10^{-13}$.
View Solution

Step 1: First Dissociation
$H_2S \rightleftharpoons H^+ + HS^-$
Since $K_{a1} \gg K_{a2}$, virtually all $H^+$ comes from the first step.
$[H^+] \approx [HS^-] = \sqrt{K_{a1}C} = \sqrt{10^{-7} \times 0.1} = \sqrt{10^{-8}} = 10^{-4} \text{ M}$.

Step 2: Second Dissociation
$HS^- \rightleftharpoons H^+ + S^{2-}$
$K_{a2} = \frac{[H^+][S^{2-}]}{[HS^-]}$

Step 3: Analyze Concentrations
From Step 1, we know $[H^+] \approx 10^{-4} \text{ M}$ and $[HS^-] \approx 10^{-4} \text{ M}$.
Substitute these into the $K_{a2}$ expression:
$1.2 \times 10^{-13} = \frac{(10^{-4})[S^{2-}]}{10^{-4}}$
The $10^{-4}$ terms cancel out completely!

Golden Rule: For any weak diprotic acid where $K_{a1} \gg K_{a2}$, the concentration of the secondary divalent anion is exactly equal to $K_{a2}$, independent of the initial acid concentration.

Answer: $[S^{2-}] = K_{a2} = 1.2 \times 10^{-13} \text{ M}$.
Problem 5: Salt Hydrolysis (Strong Acid - Weak Base)
Calculate the pH of a $0.1 \text{ M}$ solution of Ammonium Chloride ($NH_4Cl$). Given $K_b \text{ for } NH_3 = 1.8 \times 10^{-5}$ and $K_w = 1.0 \times 10^{-14}$.
View Solution

Step 1: Identify the Salt
$NH_4Cl$ is a salt of a Weak Base ($NH_4OH$) and a Strong Acid ($HCl$). Its aqueous solution will undergo cationic hydrolysis ($NH_4^+ + H_2O \rightleftharpoons NH_3 + H_3O^+$), making the solution acidic.

Step 2: Use the Hydrolysis Formula for pH
For a SA-WB salt, $pH = 7 - \frac{1}{2}(pK_b + \log_{10} C)$

Step 3: Calculate $pK_b$
$pK_b = -\log_{10}(1.8 \times 10^{-5}) = 5 - \log_{10}(1.8) = 5 - 0.255 = 4.745$.

Step 4: Substitute into pH formula
$C = 0.1 \implies \log_{10} C = -1$.
$pH = 7 - \frac{1}{2}(4.745 + (-1)) = 7 - \frac{1}{2}(3.745)$
$pH = 7 - 1.8725 = 5.127$.

Answer: The pH is $5.13$ (Acidic, as expected).
Problem 6: Salt Hydrolysis (Weak Acid - Strong Base)
Calculate the degree of hydrolysis ($h$) and the pH of a $0.05 \text{ M}$ solution of Sodium Acetate ($CH_3COONa$). Given $K_a \text{ for Acetic acid } = 1.8 \times 10^{-5}$.
View Solution

Step 1: Identify the Salt and Hydrolysis Type
$CH_3COONa$ is a WA-SB salt. It undergoes anionic hydrolysis ($CH_3COO^- + H_2O \rightleftharpoons CH_3COOH + OH^-$), making the solution basic.

Step 2: Calculate Hydrolysis Constant ($K_h$)
$K_h = \frac{K_w}{K_a} = \frac{10^{-14}}{1.8 \times 10^{-5}} = 5.55 \times 10^{-10}$.

Step 3: Calculate Degree of Hydrolysis ($h$)
Since $K_h$ is very small, $h = \sqrt{\frac{K_h}{C}}$.
$h = \sqrt{\frac{5.55 \times 10^{-10}}{0.05}} = \sqrt{1.11 \times 10^{-8}} = 1.05 \times 10^{-4}$. ($0.01\%$, approximation valid).

Step 4: Calculate pH
For a WA-SB salt, $pH = 7 + \frac{1}{2}(pK_a + \log_{10} C)$.
$pK_a = -\log_{10}(1.8 \times 10^{-5}) = 4.74$.
$\log_{10} C = \log_{10}(0.05) = \log_{10}(5 \times 10^{-2}) = 0.699 - 2 = -1.301$.
$pH = 7 + \frac{1}{2}(4.74 - 1.301) = 7 + \frac{1}{2}(3.439) = 7 + 1.72 = 8.72$.

Answer: Degree of hydrolysis $h = 1.05 \times 10^{-4}$; pH = $8.72$.
Problem 7: Salt Hydrolysis (Weak Acid - Weak Base)
What is the pH of a $0.1 \text{ M}$ solution of Ammonium Acetate ($CH_3COONH_4$) at $298 \text{ K}$? Given $K_a(CH_3COOH) = 1.8 \times 10^{-5}$ and $K_b(NH_3) = 1.8 \times 10^{-5}$. What happens to the pH if the solution is diluted to $0.01 \text{ M}$?
View Solution

Step 1: Identify the Salt
This is a WA-WB salt. Both the cation and anion hydrolyze.

Step 2: Formula for pH of WA-WB salt
$pH = 7 + \frac{1}{2}(pK_a - pK_b)$

Step 3: Analyze the unique property
Notice that the concentration ($C$) does not appear anywhere in the formula! The pH of a weak acid-weak base salt is completely independent of its concentration (assuming it is not so dilute that water's auto-ionization dominates).

Step 4: Calculate
Since $K_a = K_b = 1.8 \times 10^{-5}$, then $pK_a = pK_b = 4.74$.
$pH = 7 + \frac{1}{2}(4.74 - 4.74) = 7 + 0 = 7.0$.

Step 5: Effect of Dilution
Because the formula lacks a $C$ term, diluting the solution to $0.01 \text{ M}$ will not change the pH. It remains exactly 7.0.

Answer: pH is exactly $7.0$. Dilution does not affect the pH of a WA-WB salt.
Problem 8: The Henderson-Hasselbalch Equation (Acidic Buffer)
Calculate the pH of a buffer solution containing $0.2 \text{ M}$ Acetic acid and $0.5 \text{ M}$ Sodium Acetate. Given $pK_a$ of acetic acid is $4.74$.
View Solution

Step 1: Identify the Buffer
A mixture of a weak acid ($CH_3COOH$) and its conjugate base salt ($CH_3COONa$) forms an acidic buffer.

Step 2: Apply Henderson-Hasselbalch Equation
$pH = pK_a + \log_{10} \frac{[\text{Salt}]}{[\text{Acid}]}$

Step 3: Substitute and Calculate
$pH = 4.74 + \log_{10} \frac{0.5}{0.2}$
$pH = 4.74 + \log_{10} (2.5)$
$\log_{10}(2.5) \approx 0.398$.
$pH = 4.74 + 0.398 = 5.138$.

Answer: The pH of the buffer is $5.14$.
Problem 9: Buffer Action (Addition of Strong Acid)
To $1.0 \text{ Liter}$ of the buffer from Problem 8 ($0.2 \text{ M}$ Acetic acid and $0.5 \text{ M}$ Sodium Acetate), $0.1 \text{ moles}$ of gaseous $HCl$ is added. Assuming no volume change, calculate the new pH of the solution.
View Solution

Step 1: Understand Buffer Action
The added strong acid ($H^+$) will react completely with the basic component of the buffer (the Acetate ion, $CH_3COO^-$) to form more weak acid ($CH_3COOH$).
Reaction: $CH_3COO^- + H^+ \rightarrow CH_3COOH$.

Step 2: Stoichiometry of the Reaction
Initial moles (in $1 \text{ L}$): $[Salt] = 0.5 \text{ mol}$, $[Acid] = 0.2 \text{ mol}$.
Added $H^+ = 0.1 \text{ mol}$.
The $0.1 \text{ mol}$ of $H^+$ consumes $0.1 \text{ mol}$ of Salt and creates $0.1 \text{ mol}$ of Acid.
New $[Salt] = 0.5 - 0.1 = 0.4 \text{ M}$.
New $[Acid] = 0.2 + 0.1 = 0.3 \text{ M}$.

Step 3: Apply Henderson-Hasselbalch Equation
$pH = pK_a + \log_{10} \frac{[\text{New Salt}]}{[\text{New Acid}]}$
$pH = 4.74 + \log_{10} \frac{0.4}{0.3} = 4.74 + \log_{10}(1.33)$
$\log_{10}(1.33) \approx 0.124$.
$pH = 4.74 + 0.124 = 4.864$.

Check: The pH dropped from 5.14 to 4.86 upon adding a strong acid, demonstrating excellent buffer capacity.

Answer: The new pH is $4.86$.
Problem 10: Basic Buffer Design
You need to prepare a basic buffer of pH $10.0$. You have a $0.1 \text{ M}$ solution of Ammonia ($NH_3$, $pK_b = 4.74$) and solid Ammonium Chloride ($NH_4Cl$, Molar mass = $53.5 \text{ g/mol}$). How many grams of $NH_4Cl$ must be added to $1.0 \text{ L}$ of the $NH_3$ solution?
View Solution

Step 1: Convert pH to pOH
For a basic buffer, the equation uses pOH.
$pOH = 14.0 - pH = 14.0 - 10.0 = 4.0$.

Step 2: Apply Henderson-Hasselbalch for Basic Buffer
$pOH = pK_b + \log_{10} \frac{[\text{Salt}]}{[\text{Base}]}$
$4.0 = 4.74 + \log_{10} \frac{[\text{Salt}]}{0.1}$

Step 3: Solve for [Salt]
$\log_{10} \frac{[\text{Salt}]}{0.1} = 4.0 - 4.74 = -0.74$
$\frac{[\text{Salt}]}{0.1} = 10^{-0.74} = 0.182$
$[\text{Salt}] = 0.182 \times 0.1 = 0.0182 \text{ M}$.

Step 4: Calculate Mass of $NH_4Cl$
Since volume is $1.0 \text{ L}$, we need $0.0182 \text{ moles}$ of $NH_4Cl$.
Mass = Moles $\times$ Molar Mass = $0.0182 \text{ mol} \times 53.5 \text{ g/mol} = 0.9737 \text{ g}$.

Answer: $0.974 \text{ grams}$ of $NH_4Cl$ must be added.
Problem 11: Solubility Product ($K_{sp}$) Extraction
The solubility of Barium Sulfate ($BaSO_4$) in water at $298 \text{ K}$ is $1.05 \times 10^{-5} \text{ mol L}^{-1}$. Calculate its solubility product ($K_{sp}$).
View Solution

Step 1: Write the Dissociation Equation
$BaSO_4(s) \rightleftharpoons Ba^{2+}(aq) + SO_4^{2-}(aq)$

Step 2: Relate Solubility ($S$) to Ion Concentration
If solubility is $S$, then at equilibrium:
$[Ba^{2+}] = S$
$[SO_4^{2-}] = S$

Step 3: Write $K_{sp}$ Expression and Calculate
$K_{sp} = [Ba^{2+}][SO_4^{2-}] = (S)(S) = S^2$
$K_{sp} = (1.05 \times 10^{-5})^2 = 1.1025 \times 10^{-10}$.

Answer: $K_{sp} = 1.10 \times 10^{-10}$.
Problem 12: Common Ion Effect on Solubility
The $K_{sp}$ of $AgCl$ is $1.8 \times 10^{-10}$. Calculate the solubility of $AgCl$ in (a) pure water, and (b) in a $0.1 \text{ M}$ solution of $NaCl$.
View Solution

Part (a): Solubility in Pure Water
$AgCl(s) \rightleftharpoons Ag^+ + Cl^-$
$K_{sp} = [Ag^+][Cl^-] = (S)(S) = S^2$
$S = \sqrt{1.8 \times 10^{-10}} = 1.34 \times 10^{-5} \text{ M}$.

Part (b): Solubility in $0.1 \text{ M } NaCl$
$NaCl$ is a strong electrolyte, completely yielding $[Cl^-] = 0.1 \text{ M}$.
Let the new solubility of $AgCl$ be $S'$.
Total $[Cl^-] = 0.1 \text{ (from NaCl)} + S' \text{ (from AgCl)}$.
Since $S'$ is incredibly small, total $[Cl^-] \approx 0.1 \text{ M}$.
$K_{sp} = [Ag^+][Cl^-]$
$1.8 \times 10^{-10} = (S')(0.1)$
$S' = \frac{1.8 \times 10^{-10}}{0.1} = 1.8 \times 10^{-9} \text{ M}$.

Insight: The common $Cl^-$ ion forced the equilibrium backward, dropping the solubility of $AgCl$ by a factor of 10,000!

Answer: (a) $1.34 \times 10^{-5} \text{ M}$; (b) $1.8 \times 10^{-9} \text{ M}$.
Problem 13: Simultaneous Solubility
Solid $AgCl$ ($K_{sp} = 1.0 \times 10^{-10}$) and solid $AgBr$ ($K_{sp} = 5.0 \times 10^{-13}$) are added together to a beaker of pure water until saturated. Calculate the concentration of $Br^-$ ions in the resulting solution.
View Solution

Step 1: Set up simultaneous equilibria
Let solubility of $AgCl = x$ and solubility of $AgBr = y$.
$AgCl \rightleftharpoons Ag^+ + Cl^-$
$AgBr \rightleftharpoons Ag^+ + Br^-$
Total $[Ag^+]$ in the beaker $= x + y$.
$[Cl^-] = x$, $[Br^-] = y$.

Step 2: Write $K_{sp}$ equations
$K_{sp}(AgCl) = (x+y)x = 10^{-10}$ --- (Eq 1)
$K_{sp}(AgBr) = (x+y)y = 5 \times 10^{-13}$ --- (Eq 2)

Step 3: Analyze via approximation
Because $K_{sp}(AgCl) \gg K_{sp}(AgBr)$, $AgCl$ is vastly more soluble. Therefore, almost all the $Ag^+$ in solution comes from $AgCl$. Thus, $x \gg y$, meaning $(x+y) \approx x$.
Eq 1 simplifies to: $(x)x \approx 10^{-10} \implies x \approx 10^{-5} \text{ M}$.
Total $[Ag^+] \approx 10^{-5} \text{ M}$.

Step 4: Solve for $y$ ($Br^-$ concentration)
Substitute total $[Ag^+]$ into Eq 2:
$[Ag^+][Br^-] = 5 \times 10^{-13}$
$(10^{-5})y = 5 \times 10^{-13}$
$y = 5 \times 10^{-8} \text{ M}$.

Answer: $[Br^-] = 5 \times 10^{-8} \text{ M}$.
Problem 14: Precipitation Threshold ($Q_{sp}$ vs $K_{sp}$)
$50 \text{ mL}$ of $0.02 \text{ M } BaCl_2$ is mixed with $50 \text{ mL}$ of $0.02 \text{ M } Na_2SO_4$. Will a precipitate of $BaSO_4$ form? ($K_{sp} \text{ of } BaSO_4 = 1.1 \times 10^{-10}$).
View Solution

Step 1: Calculate new concentrations after mixing
When equal volumes ($50 \text{ mL}$ each) are mixed, the total volume doubles ($100 \text{ mL}$), so concentrations are exactly halved.
New $[Ba^{2+}] = \frac{0.02}{2} = 0.01 \text{ M} = 10^{-2} \text{ M}$.
New $[SO_4^{2-}] = \frac{0.02}{2} = 0.01 \text{ M} = 10^{-2} \text{ M}$.

Step 2: Calculate Ionic Product ($Q_{sp}$)
$Q_{sp} = [Ba^{2+}][SO_4^{2-}] = (10^{-2})(10^{-2}) = 10^{-4}$.

Step 3: Compare $Q_{sp}$ with $K_{sp}$
$K_{sp} = 1.1 \times 10^{-10}$.
Since $Q_{sp} > K_{sp}$ ($10^{-4} \gg 10^{-10}$), the solution is massively supersaturated. To restore equilibrium, the excess ions will crash out of solution.

Answer: Yes, a heavy precipitate of $BaSO_4$ will form immediately.
Problem 15: Selective Precipitation
A solution contains $0.1 \text{ M } Cl^-$ and $0.1 \text{ M } CrO_4^{2-}$. $AgNO_3$ solution is slowly added to it. Which ion will precipitate first? What will be the concentration of the first ion when the second ion just begins to precipitate? ($K_{sp}(AgCl) = 1.8 \times 10^{-10}$, $K_{sp}(Ag_2CrO_4) = 1.1 \times 10^{-12}$).
View Solution

Step 1: Calculate $[Ag^+]$ required to start precipitation for each
For $AgCl$: $[Ag^+] = \frac{K_{sp}}{[Cl^-]} = \frac{1.8 \times 10^{-10}}{0.1} = 1.8 \times 10^{-9} \text{ M}$.
For $Ag_2CrO_4$: $[Ag^+] = \sqrt{\frac{K_{sp}}{[CrO_4^{2-}]}} = \sqrt{\frac{1.1 \times 10^{-12}}{0.1}} = \sqrt{1.1 \times 10^{-11}} = 3.3 \times 10^{-6} \text{ M}$.

Step 2: Identify first precipitate
Since $1.8 \times 10^{-9} < 3.3 \times 10^{-6}$, $AgCl$ requires less $Ag^+$ to reach its solubility limit. Thus, $AgCl$ precipitates first.

Step 3: Concentration of $Cl^-$ when $Ag_2CrO_4$ begins to precipitate
$Ag_2CrO_4$ begins precipitating exactly when $[Ag^+]$ reaches $3.3 \times 10^{-6} \text{ M}$.
At this specific $[Ag^+]$, what is the $[Cl^-]$ forced to be by the $AgCl$ equilibrium?
$[Cl^-] = \frac{K_{sp}(AgCl)}{[Ag^+]} = \frac{1.8 \times 10^{-10}}{3.3 \times 10^{-6}} = 5.45 \times 10^{-5} \text{ M}$.

Insight: The $[Cl^-]$ dropped from $0.1 \text{ M}$ to $0.0000545 \text{ M}$ before the chromate even started precipitating. This proves $>99.9\%$ of the chloride can be separated cleanly!

Answer: $AgCl$ precipitates first. $[Cl^-]$ remaining is $5.45 \times 10^{-5} \text{ M}$.
Problem 16: Complexation Boosting Solubility
Calculate the solubility of $AgCl$ ($K_{sp} = 1.8 \times 10^{-10}$) in a $1.0 \text{ M}$ aqueous solution of Ammonia ($NH_3$). The formation constant ($K_f$) of the complex $[Ag(NH_3)_2]^+$ is $1.6 \times 10^7$.
View Solution

Step 1: Combine the two simultaneous equilibria
Dissolution: $AgCl(s) \rightleftharpoons Ag^+ + Cl^-$ $\quad (K_{sp})$
Complexation: $Ag^+ + 2NH_3 \rightleftharpoons [Ag(NH_3)_2]^+$ $\quad (K_f)$
Overall Net Reaction: $AgCl(s) + 2NH_3 \rightleftharpoons [Ag(NH_3)_2]^+ + Cl^-$

Step 2: Calculate overall equilibrium constant ($K_{net}$)
When equations are added, constants are multiplied.
$K_{net} = K_{sp} \times K_f = (1.8 \times 10^{-10}) \times (1.6 \times 10^7) = 2.88 \times 10^{-3}$.

Step 3: Setup ICE Table for the overall reaction
Let solubility be $S$.
Initial $[NH_3] = 1.0 \text{ M}$. Products = $0$.
Equilibrium $[NH_3] = 1.0 - 2S$.
Equilibrium $[[Ag(NH_3)_2]^+] = S$.
Equilibrium $[Cl^-] = S$.

Step 4: Solve for S
$K_{net} = \frac{S \cdot S}{(1.0 - 2S)^2} = \frac{S^2}{(1.0 - 2S)^2}$
$2.88 \times 10^{-3} = \left( \frac{S}{1.0 - 2S} \right)^2$
Take the square root of both sides ($\sqrt{0.00288} \approx 0.0537$):
$0.0537 = \frac{S}{1.0 - 2S}$
$0.0537 - 0.1074S = S$
$1.1074S = 0.0537 \implies S = 0.0485 \text{ M}$.

Answer: Solubility is $0.0485 \text{ M}$ (Massively increased from pure water's $1.34 \times 10^{-5} \text{ M}$!).
Problem 17: pH of an Amphoteric Salt
Calculate the pH of a $0.1 \text{ M}$ solution of Sodium Bicarbonate ($NaHCO_3$). For carbonic acid ($H_2CO_3$), $K_{a1} = 4.3 \times 10^{-7}$ and $K_{a2} = 5.6 \times 10^{-11}$.
View Solution

Step 1: Understand Amphoteric nature of $HCO_3^-$
The bicarbonate ion can act as an acid (donating its proton to become $CO_3^{2-}$) or as a base (accepting a proton to become $H_2CO_3$).

Step 2: Formula for ampholyte pH
For an intermediate amphoteric ion derived from a polyprotic acid, the pH is practically independent of concentration and is given by the average of the two relevant $pK_a$ values:
$pH = \frac{pK_{a1} + pK_{a2}}{2}$

Step 3: Calculate the $pK_a$ values
$pK_{a1} = -\log_{10}(4.3 \times 10^{-7}) = 7 - \log_{10}(4.3) = 7 - 0.633 = 6.367$
$pK_{a2} = -\log_{10}(5.6 \times 10^{-11}) = 11 - \log_{10}(5.6) = 11 - 0.748 = 10.252$

Step 4: Calculate pH
$pH = \frac{6.367 + 10.252}{2} = \frac{16.619}{2} = 8.31$.

Answer: The pH is $8.31$ (mildly basic).
Problem 18: Mixture of Strong and Weak Acids
Calculate the $[H^+]$ and $[CN^-]$ in a solution that is $0.1 \text{ M}$ in $HCl$ and $0.1 \text{ M}$ in $HCN$ ($K_a = 4.0 \times 10^{-10}$).
View Solution

Step 1: Analyze Total $[H^+]$
$HCl$ is a strong acid and dissociates $100\%$, providing $[H^+] = 0.1 \text{ M}$.
$HCN$ is a very weak acid. Its dissociation is heavily suppressed by the common ion effect from the strong $HCl$.
Total $[H^+] = 0.1 \text{ (from HCl)} + x \text{ (from HCN)} \approx 0.1 \text{ M}$.

Step 2: Calculate $[CN^-]$
Write the equilibrium for $HCN$: $HCN \rightleftharpoons H^+ + CN^-$
$K_a = \frac{[H^+][CN^-]}{[HCN]}$
Substitute the total $[H^+]$ from the strong acid:
$4.0 \times 10^{-10} = \frac{(0.1)[CN^-]}{0.1}$

Step 3: Solve
The $0.1$ cancels out perfectly on the right side.
$[CN^-] = 4.0 \times 10^{-10} \text{ M}$.

Answer: $[H^+] = 0.1 \text{ M}$; $[CN^-] = 4.0 \times 10^{-10} \text{ M}$.
Problem 19: Titration Curve (pH at Equivalence Point)
$50 \text{ mL}$ of $0.1 \text{ M}$ Acetic acid ($K_a = 1.8 \times 10^{-5}$) is titrated with $0.1 \text{ M } NaOH$. Calculate the pH precisely at the equivalence point.
View Solution

Step 1: Identify Equivalence Point Chemistry
At equivalence, all $CH_3COOH$ is neutralized to $CH_3COONa$.
Volume of $0.1 \text{ M } NaOH$ required to neutralize $50 \text{ mL}$ of $0.1 \text{ M }$ acid is exactly $50 \text{ mL}$.
Total volume = $50 + 50 = 100 \text{ mL}$.

Step 2: Calculate Concentration of the Salt
Moles of salt formed = Moles of acid initially present = $0.1 \text{ M} \times 0.05 \text{ L} = 0.005 \text{ mol}$.
New concentration $C = \frac{0.005 \text{ mol}}{0.100 \text{ L}} = 0.05 \text{ M}$.

Step 3: Apply Salt Hydrolysis Formula
$CH_3COONa$ is a WA-SB salt. The solution is basic.
$pH = 7 + \frac{1}{2}(pK_a + \log_{10} C)$
$pK_a = -\log_{10}(1.8 \times 10^{-5}) = 4.74$
$\log_{10}(0.05) = \log_{10}(5 \times 10^{-2}) = 0.699 - 2 = -1.301$
$pH = 7 + \frac{1}{2}(4.74 - 1.301) = 7 + \frac{1}{2}(3.439) = 7 + 1.72 = 8.72$.

Answer: pH exactly at the equivalence point is $8.72$.
Problem 20: Acid-Base Indicator Range
An acid-base indicator ($HIn$) has a $K_{In} = 1.0 \times 10^{-5}$. The un-ionized form is Red, and the ionized form ($In^-$) is Blue. Calculate the exact pH range over which the indicator visibly changes color.
View Solution

Step 1: Understand Indicator Theory
An indicator is just a weak acid: $HIn \rightleftharpoons H^+ + In^-$.
By Henderson-Hasselbalch: $pH = pK_{In} + \log_{10}\frac{[In^-]}{[HIn]}$.
The human eye perceives a complete color change when one form is at least 10 times more concentrated than the other.

Step 2: Calculate Limits
Red limit: $[HIn]$ is 10x greater than $[In^-]$. Ratio $= 1/10$.
$pH_{red} = pK_{In} + \log_{10}(1/10) = pK_{In} - 1$.
Blue limit: $[In^-]$ is 10x greater than $[HIn]$. Ratio $= 10/1$.
$pH_{blue} = pK_{In} + \log_{10}(10) = pK_{In} + 1$.

Step 3: Calculate Range
$pK_{In} = -\log_{10}(10^{-5}) = 5.0$.
Range $= (5.0 - 1)$ to $(5.0 + 1)$.

Answer: The visible color change pH range is $4.0 \text{ to } 6.0$.
Problem 21: Thermodynamics of Water Ionization
At $373 \text{ K} (100^{\circ}\text{C})$, the ionic product of water ($K_w$) is $1.0 \times 10^{-12}$. Calculate the pH of pure neutral water at this temperature. Is the water acidic?
View Solution

Step 1: Calculate $[H^+]$ in pure water
In pure water, auto-ionization produces equal amounts of $H^+$ and $OH^-$.
$[H^+] = [OH^-] = \sqrt{K_w}$
$[H^+] = \sqrt{1.0 \times 10^{-12}} = 1.0 \times 10^{-6} \text{ M}$.

Step 2: Calculate pH
$pH = -\log_{10}(1.0 \times 10^{-6}) = 6.0$.

Step 3: Analyze Acidic/Neutral Concept
Even though the pH is 6.0, the water is strictly Neutral. The definition of neutrality is not "pH = 7", but rather $[H^+] = [OH^-]$. Since both are equal at $10^{-6} \text{ M}$, it remains neutral. The entire pH scale shifts downwards at higher temperatures because the auto-ionization of water is an endothermic process.

Answer: pH is $6.0$. The water is Neutral.
Problem 22: Designing a Buffer (Volumetric Mixing)
What volume of $0.2 \text{ M } NaOH$ must be added to $100 \text{ mL}$ of $0.5 \text{ M }$ Formic acid ($pK_a = 3.74$) to prepare a buffer of pH $4.04$?
View Solution

Step 1: Reaction Stoichiometry
Let $V$ be the volume of $NaOH$ added in mL.
Initial millimoles of $HCOOH = 100 \times 0.5 = 50 \text{ mmol}$.
Added millimoles of $NaOH = V \times 0.2 = 0.2V \text{ mmol}$.
The $NaOH$ converts $HCOOH$ into $HCOONa$ (Salt).
Moles of Salt formed $= 0.2V$.
Moles of Acid remaining $= 50 - 0.2V$.

Step 2: Apply Henderson-Hasselbalch
$pH = pK_a + \log_{10} \frac{[\text{Salt}]}{[\text{Acid}]}$
Since they share the same total volume, we can use the ratio of millimoles directly.
$4.04 = 3.74 + \log_{10} \frac{0.2V}{50 - 0.2V}$

Step 3: Solve for V
$0.30 = \log_{10} \frac{0.2V}{50 - 0.2V}$
Taking antilog ($10^{0.30} \approx 2.0$):
$2.0 = \frac{0.2V}{50 - 0.2V}$
$100 - 0.4V = 0.2V$
$0.6V = 100 \implies V = \frac{100}{0.6} = 166.67 \text{ mL}$.

Answer: $166.67 \text{ mL}$ of $NaOH$ must be added.
Problem 23: Solubility of Weak Acid Salts in Buffers
Calculate the solubility of Calcium Fluoride ($CaF_2$, $K_{sp} = 4.0 \times 10^{-11}$) in a heavily buffered solution of pH = 3.0. Given $K_a \text{ for HF} = 7.2 \times 10^{-4}$.
View Solution

Step 1: Understand the Double Equilibrium
$CaF_2$ dissolves: $CaF_2 \rightleftharpoons Ca^{2+} + 2F^-$.
Because $F^-$ is the conjugate base of a weak acid, it reacts with the abundant $H^+$ in the buffer: $F^- + H^+ \rightleftharpoons HF$.
The $H^+$ pulls the $F^-$ out of the solubility equilibrium, forcing more $CaF_2$ to dissolve!

Step 2: Establish Mass Balance
Let solubility be $S$. Then total Calcium is $S$, and total Fluorine species ($F^-$ + $HF$) is $2S$.
$[Ca^{2+}] = S$
$[F^-] + [HF] = 2S$

Step 3: Relate $[F^-]$ to $[HF]$ using $K_a$
$K_a = \frac{[H^+][F^-]}{[HF]} \implies [HF] = \frac{[H^+][F^-]}{K_a}$.
Substitute into mass balance:
$[F^-] + \frac{[H^+][F^-]}{K_a} = 2S \implies [F^-]\left(1 + \frac{[H^+]}{K_a}\right) = 2S$
$[F^-] = \frac{2S}{1 + \frac{[H^+]}{K_a}}$

Step 4: Substitute into $K_{sp}$ and Solve
$pH = 3.0 \implies [H^+] = 10^{-3} \text{ M}$.
Denominator factor: $1 + \frac{10^{-3}}{7.2 \times 10^{-4}} = 1 + \frac{10}{7.2} = 1 + 1.389 = 2.389$.
So, $[F^-] = \frac{2S}{2.389} = 0.837 S$.
$K_{sp} = [Ca^{2+}][F^-]^2 \implies 4.0 \times 10^{-11} = (S)(0.837 S)^2$
$4.0 \times 10^{-11} = 0.70 S^3$
$S^3 = 5.71 \times 10^{-11} = 57.1 \times 10^{-12}$
$S = (57.1)^{1/3} \times 10^{-4} \approx 3.85 \times 10^{-4} \text{ M}$.

Answer: Solubility is $3.85 \times 10^{-4} \text{ M}$.
Problem 24: Precipitation of Metal Hydroxides
Calculate the minimum pH required to prevent the precipitation of $ZnS$ ($K_{sp} = 1.0 \times 10^{-21}$) from a solution containing $0.01 \text{ M } Zn^{2+}$ saturated with $H_2S$ ($0.1 \text{ M}$). For $H_2S$, $K_{a1} \times K_{a2} = 1.0 \times 10^{-21}$.
View Solution

Step 1: Find maximum allowed $[S^{2-}]$
To just prevent precipitation, $Q_{sp} \le K_{sp}$.
$[Zn^{2+}][S^{2-}] = 1.0 \times 10^{-21}$
$(0.01)[S^{2-}] = 1.0 \times 10^{-21} \implies [S^{2-}] = 1.0 \times 10^{-19} \text{ M}$.

Step 2: Relate $[S^{2-}]$ to $[H^+]$ using overall $K_a$
For the overall dissociation $H_2S \rightleftharpoons 2H^+ + S^{2-}$:
$K_{overall} = K_{a1} \times K_{a2} = \frac{[H^+]^2[S^{2-}]}{[H_2S]}$

Step 3: Solve for $[H^+]$
$1.0 \times 10^{-21} = \frac{[H^+]^2 (1.0 \times 10^{-19})}{0.1}$
$[H^+]^2 = \frac{1.0 \times 10^{-22}}{1.0 \times 10^{-19}} = 1.0 \times 10^{-3}$
$[H^+] = \sqrt{10 \times 10^{-4}} = 3.16 \times 10^{-2} \text{ M}$.

Step 4: Calculate pH
$pH = -\log_{10}(3.16 \times 10^{-2}) = 2 - \log_{10}(3.16) = 2 - 0.5 = 1.5$.
If the pH is kept below 1.5 (highly acidic), the $S^{2-}$ concentration stays suppressed below the precipitation threshold.

Answer: Maximum pH to prevent precipitation is $1.5$.
Problem 25: Master Challenge - Simultaneous Equilibria
What is the degree of hydrolysis of $0.1 \text{ M } KCN$ solution? Given $K_a(HCN) = 4.0 \times 10^{-10}$. What happens to the degree of hydrolysis if this solution is mixed with an equal volume of $0.1 \text{ M } NH_4Cl$ ($K_b(NH_3) = 1.8 \times 10^{-5}$)?
View Solution

Part 1: Pure KCN Solution
$KCN$ is a WA-SB salt. It undergoes anionic hydrolysis ($CN^- + H_2O \rightleftharpoons HCN + OH^-$).
$K_h = \frac{K_w}{K_a} = \frac{10^{-14}}{4.0 \times 10^{-10}} = 2.5 \times 10^{-5}$.
$h = \sqrt{\frac{K_h}{C}} = \sqrt{\frac{2.5 \times 10^{-5}}{0.1}} = \sqrt{2.5 \times 10^{-4}} = 1.58 \times 10^{-2}$ (or $1.58\%$).

Part 2: Mixing with $NH_4Cl$
When mixed, you have a mixture of a weak acid anion ($CN^-$) and a weak base cation ($NH_4^+$). They will mutually hydrolyze each other in a process called mutual hydrolysis.
Reaction: $NH_4^+ + CN^- \rightleftharpoons NH_3 + HCN$.
The equilibrium constant for this mutual reaction ($K_{mut}$) is much larger than individual $K_h$.
$K_{mut} = \frac{K_w}{K_a \times K_b} = \frac{10^{-14}}{(4.0 \times 10^{-10})(1.8 \times 10^{-5})} = \frac{10^{-14}}{7.2 \times 10^{-15}} = \frac{10}{7.2} = 1.38$.

Because $K_{mut}$ is huge compared to standard hydrolysis constants ($10^{-5}$), the reaction goes forward aggressively. The degree of hydrolysis ($h$) jumps from a mere $1.58\%$ to a massive percentage!

Calculate new $h$:
$K_{mut} = \frac{h^2}{(1-h)^2} \implies \frac{h}{1-h} = \sqrt{1.38} = 1.175$.
$h = 1.175 - 1.175h \implies 2.175h = 1.175 \implies h = 0.54$ (or $54\%$).

Answer: Initial hydrolysis is $1.58\%$. Upon mixing, mutual hydrolysis massively boosts it to $54\%$.

Mastering the Math of Acids and Bases

Congratulations on completing these 25 highly advanced numericals on Ionic Equilibrium. By conquering simultaneous solubilities, exact polyprotic derivations, the mathematical nuance of buffer capacity, and the extreme limits of the common ion effect, you have built the ultimate foundation for all of physical chemistry. Remember that in equilibrium, mastering the approximations—knowing exactly when to ignore a tiny '$x$' and when to solve the full quadratic—is the true mark of a JEE Advanced scholar!

Frequently Asked Questions (FAQs)

Q1. When can I safely ignore '$x$' in a weak acid calculation?
A standard rule of thumb is the $5\%$ rule. If the calculated degree of dissociation ($\alpha$) using the simplified approximation formula ($\alpha = \sqrt{K_a/C}$) comes out to be less than $0.05$ (or $5\%$), the approximation is valid. If it is greater than $5\%$, you must solve the full quadratic equation $K_a = \frac{C\alpha^2}{1-\alpha}$.
Q2. Why is the pH of a strong acid like $10^{-8} \text{ M HCl}$ not 8?
Acids, by definition, must yield a pH of less than 7 at $298 \text{ K}$ in water. When the concentration of added acid is exceptionally small (near or below $10^{-7} \text{ M}$), the $H^+$ ions naturally contributed by the auto-ionization of water ($10^{-7} \text{ M}$) can no longer be ignored. You must sum both sources of $H^+$, which mathematically guarantees the pH stays slightly below 7 (e.g., 6.98).
Q3. Does diluting a buffer solution change its pH?
No, moderate dilution does not change the pH of a buffer. The Henderson-Hasselbalch equation ($pH = pK_a + \log(\text{[Salt]/[Acid]})$) relies on the ratio of concentrations. Since adding water dilutes both the salt and the acid equally, their ratio remains perfectly constant, and the pH does not shift.
Q4. What is the difference between $K_{sp}$ and $Q_{sp}$?
$K_{sp}$ (Solubility Product Constant) is a strict equilibrium value at a given temperature that indicates the maximum possible concentration of ions before a solid forms. $Q_{sp}$ (Ionic Product) is the product of ion concentrations at any given moment. If $Q_{sp} > K_{sp}$, the solution is supersaturated and precipitation will occur to restore equilibrium.
Q5. Why does $AgCl$ dissolve in ammonia?
Ammonia ($NH_3$) acts as a powerful ligand that forms a highly stable complex ion ($[Ag(NH_3)_2]^+$) with free $Ag^+$ ions. This complexation process rapidly removes $Ag^+$ from the aqueous solution. According to Le Chatelier's Principle, the $AgCl$ solid must dissolve further to try and replace the lost $Ag^+$ ions, massively increasing its overall solubility.
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